The elemental content of 61 raw propolis samples from Pest, Zala and Bács-Kiskun county (Hungary) were analyzed by ICP-OES. The content of Al, B, Ca, Cu, Fe, K, Mg, Mn, Na, P, S, Sr and Zn were measured in the samples. Median is higher than mean in all cases based on the summarized results. It can be explained by the outliers, moreover it has a non-normal distribution. The concentrations are in an extremely wide range, the ratio of the maximum and minimum is under 10 in case of six elements, between 10 and 35.1 in the case of other six elements,and more than 300 in case of Zn. Significant differences are between counties only in the case of B, K and P based on ANOVA. Other elements have no significant differences. The following order can be set up based on the mean concentrations and the wide ranges: K≥Ca>P≥S≥Fe≥Mg≥Al>Zn≥Na>Mn≥B>Cu≥Sr. Moreover it can be established, that the measured concentrations are near the same or in some cases lower than in other publications.
The wool of sheep is suitable to test the mineral supply; however, a number of factors could affect the results. The growth rate and length of staple can be very different according to season, physiological state and individual variation. These factors are likely to affect the quantity of minerals accumulated into the wool. Therefore, the purpose of this research was to examine whether there is a difference between the mineral content of wool nearly reached the full staple length and the freshly grown wool using the same feeding regime.
10 Tsigai pregnant sheep have been selected randomly from the same farm. Wool samples were obtained from the withers, side and quarter with bended scissors. Samples were mineralized using nitric acid and hydrogen peroxide using ultrasonic cleaning unit. P, Ca, Mg, Na, S, Cu,Se and Zn content were determined by ICP-OES. Statistical analyses were carried out by SAS (SAS Institute Inc., Cary, NC) GLM procedure.Differences between means were tested by Tukey test. Significantly lower Ca, Na, P, Zn values were found in case of intensively grown wool. Sampling location did not affect the mineral content. Herd mineral supply was adequate. Our results suggest that intensively grown wool samples have to be used for mineral analyses.
Mineral supplementation is very important in high producing farm animals. The estimation of exact mineral intake is very difficult in forage eating animals, like sheep. Accessing of long term mineral status seems to be possible using wool mineral analysis. However several factors can affect the results. Therefore, the aim of this study was to test the effect of breed and sampling location on the mineral content of sheep wool. 20 Dorper and 20 Tsigai sheep were chosen from the same farm. Samples were obtained from 3 locations (withers, side and quarter) and tested for 8 elements: Ca, Mg, Na, Co, Cu, P, S, Se , Zn. The samples were cleaned with ethyl alcohol from organic contamination, then after adding nitric acid were mineral analized using ultrasonic cleaning unit. The samples were analysed with ICP-OES (Perkin-Elmer, Optima 3300 DV). Statistical analyses were carried out by GLM procedure of SAS statistical analyses software. Differences between means were checked with Tukey-test. Significant breed differences were detected in the case of Mg, Na, S, Se in spite of the same feeding regime. The wool mineral content were within the reference range. The sampling location had no effect on the mineral content of wool.
The level of mineral elements is important factor regarding the quality of milk. The aim of our research study was to determine the content of mineral elements in milk of Holstein, Jersey, Brown Swiss, Ayrshire, Norwegian-red, Swedish-red cows in the first stage of lactation. All cows were fed with the same type (composition) of feed and they were kept under the same condition. The concentration of macroelements (K, Na, Ca, P, Mg, S) in digested milk samples was determined by inductively coupled plasma optical emission spectrometry (ICP-OES).
Molybdenum is not a well-known microelement, but being a constituent of several important cellular enzymes it is an essential microelement. Molybdenum occurs in all foods, but at very low levels. There does not appear to be any particular foods or types of foods, which in the absence of extrinsic factors, naturally have high levels of molybdenum. However, environmental pollution, from natural or anthropogenic sources, can lead to high level of the metal in plants.
Our study is based on the long-term field experiments of Nagyhörcsök, where different levels of soil contamination conditions are simulated. Soil and plant samples were collected from the experiment station to study the behaviour of molybdenum: total concentration, available concentration, leaching, transformation, uptake by and transport within the plants, accumulation in different organs, phytotoxicity and effects on the quantity and quality of the crop. In this work we present the results of maize and peas and the soil samples related to them.
According to our data molybdenum is leaching from the topsoil at a medium rate and it appears in the deeper layers. In the case of plant samples we found that molybdenum level in the straw is many times higher than that is in the grain, so molybdenum accumulates in the vegetative organs of the plant. The data also show differences in the molybdenum-uptake of cereals and Fabaceae (or Leguminosae).
The yield and quality of the sugar beet are mainly determined by level crop production system; therefore the effects of foliar fertilization were studied. Our field trials were carried out in 2005 and 2006 in Hajdúböszörmény, at two experimental sites. In our trials the effects of Biomit Plussz, Fitohorm and Kelcare Cu (having high Cu content) as foliar fertilizers, as well as a fungicide with high sulphur content, Cosavet DF, were studied and
compared. Effects of treatments were studied in four replicates.
We took root samples at 4 week intervals, starting in August. The quality of root (sucrose, potassium, sodium and alfa-amino N content) was determined from filtrated beet broth, by an automatic beet laboratory system, called VENEMA. Leaf samples were taken three times in the growing season, element composition was measured by ICP-OES.
We found that the crop and the sugar yield were significantly influenced by the foliar treatments both of the two years.
Six macroelements and twelve microelements were identified in thirty-six Hungarian acacia honeys collected from ten counties by inductively coupled plasma optical emission spectrometry (ICP-OES) and inductively coupled plasma mass spectrometry (ICP-MS). One-Way ANOVA (LSD and Dunnett T3 test) and linear discriminant analysis (LDA) were used to determine the statistically verified differences among the honey samples with different geographical origin.
Significant differences were established among the samples from different counties in Na, P, S, Fe, Ni, Cu and Sr concentrations. Based on the macroelement content of honeys, the separation of samples with different geographical origin was not successful because the percent of correctly categorised cases was only 64.9%. However, examining the As, B, Ba, Cu, Fe Mn, Ni and Sr concentration, the separation of different groups was convincing since the percent of correctly classified cases was 97.2%. Thus, the examination of microelement concentration may be able to determine the geographical origin of acacia honeys.
The yield and quality of the sugar beet are mainly determined by the plant production system, thus we studied the effect of mineral fertilization. Our field trials were carried out in 2005 and 2006 in Hajdúböszörmény, at two sites. We studied the effect of sulphur (Cosavet DF), copper (Kelcare Cu) and two foliar nutrients with high active agents. Treatments were replicated four times.
We took root and leaf samples at 4 week intervals, starting in August. The quality of root (sucrose, potassium, sodium and alfaamino N content) was determined from filtrated beet broth, by an automatic beet laboratory system, called VENEMA. Leaf samples were measured with ICP-OES.
We found that the crop and the sugar yield were significantly influenced by the foliar treatments.
We have started a small parcell and a factorial S fertilization experiment with winter wheat in the 2001/2002 cropping year to examine its effect on yield and quality. The scene of experiment was the Latokep Experimental Station of the DE ATC (calcareous chernozeem) in case of small parcell examination and the Agricultural Company of Felsőzsolca (brown forest soil) in case od factorial examination.
The protein and gluten content of the grain was investigated with PerCon Inframatic 9001 NIR Analyser, then we have measured these parameters with PerCon 8620 infra appliance. After the milling we measured the following parameters: glutenindex, farinographic parameters (farinographic index, water absorption capacity, dough development time, stability, softening, extension) and valorigraphic index.
Based on the results there’s no justified relation between the fertilization and the protein and gluten content. The valorigraphic index of the samples taken from Felsőzsolca factory characteristically increased as a result of the S-fertilization. In the small-parcell experiment the values of the water absorption capacity, the dough development time and the softening parameters from the valorigrphic parameters depended significantly from the mineral treatments. Signifikant quality improvement wasn’t experieced.
There was sampling in all of critical phenophase (…). The green plant samples were examined on element content with ICP-OES. These measurements are currently in progress.