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Effects of long-term K fertilization and liming on the extractable and exchangeable K contents of a Haplic Phaeosem soil
Published October 5, 2010

Effects of regular K fertilization and liming on the easily extractable K content of a Haplic phaeosem soil determined in 0.01 M CaCl2
and AL (traditional method in Hungary) were examined in the B1740 type of the National Uniformed Long-Term Fertilization Experiments
at Karcag.
Close correlation (r=0.95) was found between the 0.01 M Ca...Cl2 and ammonium lactate - acetic acid (AL) extractable K contents of
K fertilization increased the amount of 0.01 M CaCl2 and AL extractable K significantly. Liming had different effects on the amounts of
K extracted by these two methods. Liming increased the amount of AL-K and decreased the amount of CaCl2-K. CaCl2 extractable K was in
close correlation with the relative amount of exchangeable K content of the soil (K%) and the agronomic K balance. The results of regression
analysis confirmed that the CaCl2-K characterized K% and the AL-K related to the absolute amount of exchangeable K.
On the basis of the presented results it can be stated that the 0.01 M CaCl2 is able to detect not just the increase of easily extractable K
caused by fertilization and liming but the changing of the rate of the relative amount of exchangeable K.

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Fertilisation Effect on Quantity of 0.01 M CaCl2 Soluble N-Forms in a Long-Term-Small-Plot Experiment
Published May 11, 2003

long-term experiments have an opportunity to investigate the effects of fertilization and plant nutrition. The paper reports the results achieved in the 39th years of a long-term-small-plot fertilisation and liming experiment set up on acidic sandy brown forest soil in the Nyírség region. From the 32 treatment, four replications, altogether 1...28 plot experiments with 10 treatments are summarized. We took samples after harvest of triticale, in August.
We used a reliable method (segmented continuous flow analysis) to determine different (easily mobilized - 0.01 M CaCl2 soluble) N-forms of soil. The 0.01 M CaCl2 soluble inorganic and total N content and the UV digestable organic-N form of soil were determined by this method.
The results are summarized below:
– The mineralized-N (Nmin.) content of soil increased with dose of nitrogen treatment. Liming treatments increase the amount of Nmin.
– The maximum content of easily mobilize organic-N-fraction was found in the upper (0-20 cm) layer. This fact due to the large amount of crop and roots.
– Changing of content of 0.01 M CaCl2 soluble total-N-forms due to N doses.
– The ratios of these N forms are variable. It is very important that the content of organic N fraction is not negligible and this fraction plays a main role in the plant nutrition.

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Study of factors controlling the amount of 0.01 M CaCl2 extractable Norg fraction
Published September 5, 2018
The use of new methods describing the “readily available” nutrient content of the soil is spreading on a global scale. The 0.01 M CaCl2 extractant is a dilute salt solution in which the easily soluble inorganic (nitrate-N and ammonium-N) and organic N fractions, P, K and micronutrients are also measurable. The 0.01 M CaCl2 has been tested... in the University of Debrecen, Institute of Agricultural Chemistry and Soil Sciences since the 90’s. The results of the researches related to organic N fraction, performed in the last decades, and the results of the present study (originating from the long-term experiment of Karcag, 2007–2009) can be concluded as follows:
The measurement of easily soluble and oxidizable organic nitrogen (Norg), besides inorganic fractions, could improve the nutrient management.
The amount of the Norg fraction is determined by the soil conditions, therefore it is considered to be a site-specific parameter.
Management practices and cropyear affect the amount of Norg as well. The present research confirmed that, the effect of fertilization on the amount of Norg can be explained by the changing of the yield (related to total biomass production), while the effect of cropyear is related to the differences in mineralization circumstances and yield as well.
The measurement of the Norg fraction is increases the accuracy of N-supply, therefore it could prevent the environmentally harmful excess N application as well.
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Studies of the influences of different N fertilizers and Microbion UNC bacterial fertilizer on the nutrient content of soil
Published October 5, 2010

A field experiment was conducted to examine the effects of different nitrogen fertilizers in combination with bacterial fertilizer on
nutrient uptake of horseradish and plant available nutrients of the soil. Three different N fertilizers, ammonium-nitrate, urea and calciumnitrate
(116 kg ha-1 N) in combination with Microbion UNC bacterial... fertilizer (2 kg ha-1) were applied as treatments in a randomized
complete block design in three replications. In this paper we presented the results of soil measurements. The soil of the experimental area
was chernozem with medium sufficiency level of N and P and poor level of K.
Our main results:
The amount of 0.01M CaCl2 soluble inorganic nitrogen fractions, NO3
--N and NH4
+-N and also the quantity of soluble organic-N were
almost the same in the soil. N fertilizers significantly increased all the soluble N fractions. The amount of NO3
--N increased to the greatest
extent and the increase of organic N was the slightest. We measured the largest CaCl2 soluble NO3
- -N and total-N contents in the plots
treated with ammonium-nitrate, the largest NH4
+-N in the plots treated with calcium-nitrate and the largest organic-N fraction in plots
treated with urea.
Bacterial inoculation also increased both soluble inorganic nitrogen forms and also total-N content of soil compared to the control. In
the case of combined (artificial and bacterial fertilizer) treatments we measured lower NO3
--N, organic-N and total-N compared to the
values of plots having only nitrogen fertilizer treatments. On the contrary in the plots with combined treatments the CaCl2 soluble NH4
content of soil in more cases were higher than that of values with artificial fertilizer treatment.
As a function of calcium-nitrate application increased AL-P2O5 and AL-K2O values were measured compared to control. Microbion
UNC supplement of calcium nitrate yielded also increase in AL-P2O5 and AL-K2O values, till then supplement of ammonium-nitrate fertilizer
yielded a decrease in these values compared to the control.
All nitrogen fertilizers resulted in a significant decrease in AL-Mg content of soil compared to the control. Nevertheless bacterial
fertilizer increased AL-Mg values in any cases.

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Preliminary Critical P-limit Values of 0.01 M CaCl2 Soil Test Procedure
Published December 4, 2001

In the last decade, the 0.01 M CaCl2 extraction procedure was tested as a multi-nutrient extractant. In 1995-97, international joint research activities were carried out within the COPERNICUS project. Detailed calibration of conventional and the 0.01 M CaCl2 extraction procedures for pH, Mg and K were published.
The amo...unt of phosphorus extracted using a 0.01 M CaCl2 solution is very low and reflects the intensity parameter of phosphorus bio-availability. As a readily desorbed P fraction of soils can reflect the soil P-supply and the CaCl2-P values are in close correlation with P-fertiliser rates and P balance. However, the effects of various soil characteristics on CaCl2-P values are different and their interpretation is difficult.
Relatively poor correlations were found between amounts of P extracted by conventional and CaCl2 soil test methods and, therefore, P limit values could not be calculated directly. To characterise the soil P supply at different sites, the CaCl2 desorbed P and the adsorbed P in a modified Baker Soil Test were also applied.
Soil test results of Hungarian long-term fertiliser experiments and recommended CaCl2-P limit values, calculated on yield effects and soil characteristics, are discussed.

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Nitrogen Supplying Capacity of Brown Forest Soil under Different Cropping Practices and 0.01 M CaCl2 Soluble Organic Nitrogen
Published October 11, 2006

The best known and most remarkable example of continuous production in Hungary is the Westsik’s crop rotation experiment, which was established in 1929, and is still in use to study the effects of organic manure treatment, to develop models, and predict the likely effects of different cropping systems on soil properties and crop yields. In respect, Westsik’s crop rotation experiment provides data of immediate value to farmers concerning the applications of green, straw and farmyard manure, as well as data sets for scientific research.
Although commonly ignored, the release of nitrogen by root and green manure crops has a significant impact on soil organic matter turnover. The design of sustainable nitrogen management strategies requires a better understanding of the processes influencing nitrogen supplying capacity, as the effects of soil organic matter on soil productivity and crop yield are still very uncertain and require further research. In the treatments of Westsik’s crop rotation experiment, nutrients removed from soil through plant growth and harvesting are replaced either by fertilisers and/or organic manure. Data can be used to study the nitrogen supplying capacity of soil under different cropping systems and its effect on the 0.01 M CaCl2 soluble organic nitrogen content of soil.
The aim of this paper is to present data on the nitrogen supplying capacity of brown forest soil from Westsik’s crop rotation experiment and to study its correlation with hundredth molar calcium-chloride soluble organic nitrogen. The main objective is to determine the effects of root and green manure crops on the nitrogen supplying capacity of soil under different cropping systems. The nitrogen supplying capacity was calculated as a difference of plant uptake, organic manure and fertiliser supply.
The 0.01 M CaCl2 soluble organic nitrogen test has proved reliable for determining the nitrogen supplying capacity of soils. Brown forest soils are low in organic matter and in the F-1 fallow-rye-potato rotation, the nitrogen supplying capacity was 15.6 kg/ha/year. 0.01 M CaCl2 soluble organic nitrogen content was as low as 1.73 mg/kg soil. Roots and green manure increased the nitrogen supplying capacity of soil by more than 100%. This increase is caused by lupine, a legumes crop, which is very well adapted to the acidic soil conditions of the Nyírség region, and cultivated as a green or root manure crop to increase soil fertility.

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The possibility of use of the 0,01 M CaCl2 and Baker- Amacher extractants for the determination of plantavailable potassium
Published November 2, 2009

The Hungarian fertilizing recommendation systems use AL soil test for the evaluation of potassium supply. The 0.01 M CaCl2 is a definitely milder extractant, it extracts the easily soluble and exchangeable potassium amount. Its European introduction was already taken into consideration in 1994. The research project on this topic is s...tarted in several european countries, also in Hungary at the Department of Agricultural Chemisty of Agricultural University of Debrecen. Another advantage this multielement method is that the different element-ratios can also be calculated.
The Baker-Amacher extractant’s principle is that it contains a known amount of K, P, Mg in the CaCl2 solution. During the soil extraction adsorption and desorption process take place, so the adsorption or desorption can be calculated from the original and the final concentrations.
In this paper we introduce the results of comparing analysis of the samples (n=630) from Soil Information and Monitoring System. Our aim was to measure the use of new extractants beside conventional extractant (AL) for the evaluation of K-supply would be reasonable.
It can be stated that there is a medium close relationship (r=0.75) between AL-K and 0.01 M CaCl2-K. My calculations confirmed the results of  former examinations, and proved that the two extractants don’t extract and change the same rate of K-fractions. We found that regression  between 0.01 M CaCl2 and AL depend on texture classes, pH classes, amount of lime, and organic matter content of soils.
Comparing the relations between AL and Baker-Amacher we find relatively loose correlation (r=0.45). We stated that there are K-fixing soils among soils considered to be well supplied with potassium by AL. This might be caused by the high amount of mineral clay and the quality of mineral clay. We stated that the dK averages show that the Hungarian nutrient-supply categories characterize generally well K-supplement of soil.
It can be stated that it would be necessary to use new extractants to specify evaluation of plant available K. We found that the 0.01 M CaCl2 and Baker-Amacher extractants could complete usefully the AL procedure and could help effective potassium fertilization.

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The effect of long-term fertilization on the 0.01 M CaCl2 extractable nutrient content of a meadow soil
Published December 16, 2012

During my research, I studied the 0.01 M CaCl2 extractable NO3--N, NH4+-N, Norg, P and K contents of the soil samples originated from a long term fertilisation trial in the experimental site Hajdúböszörmény. Relationships among the soil nutrient contents, the agronomic nutrient balances... of the 2009 year, and fertilization were studied. 
From the results of the study it was concluded as follows:
– Fertilization significantly increased the CaCl2 extractable NO3--N, NH4+-N, and K contents of soil.
– Norg fraction increased as a function of the increasing yield. Hence, it can be assumed that the greater the produced yield, the more the stubble and root residues remain on the arable land. These organic residues can result significant increase in the Norg content of soils.
– The CaCl2 extractable P and K contents were compared with the calculated P and K limit values. According to these, the experimental soil has a good phosphorus and lower potassium supply capacity. These results are in accordance with the results of the conventional Hungarian fertilization recommendation system.
– It can be stated that the 0.01 M CaCl2 is able to determine not just inorganic N forms but Norg fraction as well that characterize the easily mineralizable nitrogen reserves. The results proved that AL-P and -K (ammonium lactate acetic acid, traditional Hungarian extractant) are in good agreement with the P and K reserves, but it is important from the aspect of environmental protection and plant nutrition to measure the easily soluble and exchangeable K-, and P-contents of soil. 0.01 M CaCl2 method is recommended for this.

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